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| The measurements were conducted on the GPPD diffractometer which usually involves zirconium powder cannisters as shown here. We mounted our crystals by gluing on a smaller (inverted) Zr tube sealed in the sample cannister under He exchange gas. | ![]() |
![]() | Phil is sealing the samples in He exchange gas in a glove bag at the diffractometer. |
| The GPPD diffractometer uses a displex refrigerator with a sample attached to the copper head shown above the compressor. A cold shield is then attached which shields external blackbody radiation. This stage fits into the vacuum region (you can see the o-ring gasket around the hole) and approximately 1 m below the red "floor", the neutrons can strike the sample.
The He proportional detectors are arranged in a circle around the sample at 1 m distance and scattering is detected within a angle of 15 degrees of the horizontal plane. | ![]() |
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| Alice Acatrinei and Rich setting up a data run. | ![]() |
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Phil makes the discovery that his laptop powersupply has wings! |